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MTR NMR Facility Overview

 

Bruker Avance NEO 800 MHz NMR with shielded magnet

  • Bruker Avance NEO 800 MHz NMR with shielded magnet
    Bruker Avance NEO 800 MHz NMR with shielded magnet
    5-channel console with Z-gradient amplifier, GaAs high performance/low noise preamplifiers, 2H observation/decoupling capability.
  • SampleCase autosampler for up to 24 samples with sample cooling capability to 6°C;
  • BCU II cooling unit, cools probes down to -80 °C.
  • 5 mm helium cryogenic HCN probe with 19F capability in the 1H channel, VT range -40°C to +150°C.  2 - 4 times improved sensitivity as compared to room temperature probe.
  • 3.2 mm HCN solid state MAS probe with spinning rate up to 24 kHz, VT range -80°C to +80°C.
  • Phoenix NMR 1.6 mm MAS SB  X/Y/19F/1H probe with spinning rates up to 40 kHz (spinning module size can be switched to 2.5 mm which spins up to 32 kHz).
  • Nitrogen reliquification for up to 1-year refill cycle to maximize NMR experiment time.

 

Bruker Avance NEO 600 MHz NMR with shielded magnet
Bruker Avance NEO 600 MHz NMR with shielded magnet

Bruker Avance NEO 600 MHz NMR with shielded magnet

  • 4-channel console with Z-gradient amplifier, GaAs high performance/low noise preamplifiers, 2H observation/decoupling capability.
  • SampleCase autosampler for up to 24 samples with sample cooling capability to 6 °C.
  • BCU II cooling unit, cools probes down to -80 °C.
  • 5 mm nitrogen cryogenic HCN Prodigy probe with 19F capability in the 1H channel, VT range -40 °C to +150 °C. Up to 2.5 times improved 1H sensitivity as compared to room temperature probe.
  • 5mm broad band iProbe with BB range 19F-199Hg and 17O-109Ag and VT range -150°C to +150°C. Capable of 19F{1H} or 1H{19F} NMR.

 

Bruker Avance NEO 500 MHz NMR with shielded magnet
Bruker Avance NEO 500 MHz NMR with shielded magnet

Bruker Avance NEO 500 MHz NMR with shielded magnet

  • 2-channel console with Z-gradient amplifier, GaAs high performance/low noise preamplifiers.
  • SampleCase autosampler for up to 24 samples.
  • BCU II cooling unit, cools probes down to -80°C.
  • InsightMR flow unit for reaction monitoring with VT range -5°C to +60°C.
  • 5 mm nitrogen cryogenic Prodigy probe with BB range 31P-15N and 19F capability in the 1H channel, VT range -40°C to +150°C. Up to 3 times improved X-nucleus sensitivity as compared to room temperature probe.

 

Bruker Avance III HD 500 MHz NMR
Bruker Avance III HD 500 MHz NMR

Bruker Avance III HD 500 MHz NMR

  • 2-channel console with Z-gradient amplifier, GaAs high performance/low noise preamplifiers.
  • 5 mm HX double resonance iProbe with BB range 19F-199Hg and 17O-109Ag and VT range -150 °C to +150 °C. Capable of 19F{1H} or 1H{19F} NMR.

 

Bruker Avance NEO 400 MHz solid state NMR
Bruker Avance NEO 400 MHz solid state NMR

Bruker Avance NEO 400 MHz solid state NMR

  • 4-channel console.
  • BCU II cooling unit, cools probes down to -80 °C.
  • 3.2 mm HCN MAS E-free probe with spinning rate up to 24 kHz (spinning module size can be switched to 2.5 mm which spins up to ~32 kHz), VT range -80 °C to +80 °C.

 

Bruker Avance NEO 400 MHz solid state NMR

  • 4-channel console.
  • 4 mm HRMAS HCN triple resonance probe with spinning rate up to 15 kHz, VT range -20 °C to +80 °C.
  • 2.5 mm HFXY quadrupole resonance probe with spinning rate up to 32 kHz.

 

2 x Agilent 500 MHz DDR2 NMR spectrometer

  • Two channel system for 15N to 31P and 1H/19F observe or decoupling. 
  • 5-mm gradient OneNMR Probe optimized for both X-Nucleus and 1H sensitivity equipped with Optima automated tune module for hands-free tuning (15N to 31P on low band and 1H/19F on high band channel). -120°C to +100°C sample temperature range.
  • FTS chiller down to -80°C.
  • 7600AS 96 sample robotic sample changer.
  • VnmrJ4.2 spectrometer software.

 

Bruker Avance NEO 600 MHz Solid State NMR spectrometer

  • Three channel system optimized for Sold State NMR.
  • 1.3, 3.2, and 4 mm MAS probes are available. The 1.3 and 3.2 mm probes are H/C/N whereas the 4 mm is an automated H/X iProbe.
  • BCU II for low temperature NMR down to -80C.
  • Running TopSpin 4.3.

600 MHz Bruker Avance NEO

Varian 400 MHz Infinity-Plus Solid-State NMR spectrometer

  • Three channel consoles for dual low-band and one high-band operation.
  • Wide bore magnet.
  • Variety of NMR probes including 4-mm HXY MAS, 5-mm and 6-mm HX MAS, and deuterium wideline probe. 
  • Spinsight NMR software.

 

Facility support hardware/software

  • Four Linux datastations running VnmrJ3.1 or VnmrJ4.2 for data processing.
  • 200 seat site license for Mnova NMR processing software.
  • A variety of NMR probes for triple resonance work and low-gamma nuclei.
  • 500 MHz and 1 GHz Oscilloscopes for high power tuning and instrument troubleshooting.